Record page for info:iucr:bd6b36c3-b1bd-4ff5-9998-f5d8ca0e041e

'"4,4'-Iminodipyridinium bis(hydrogen phthalate)"'

Link to article on Publisher's site

prism:eissn"1600-5368"
prism:endingpage"2153"
prism:issn"1600-5368"
prism:number"11"
prism:publicationdate"2008-11-01"
prism:publicationname"Acta Crystallographica Section E: Structure Reports Online"
prism:rightsagent"med@iucr.org"
prism:section"organic compounds"
prism:startingpage"2153"
prism:volume"64"
dc:date"2008-11-01"
dc:description"In the title salt, C10H11N32+.2C8H5O4-, doubly protonated 4,4'-dipyridylamine (dpa) cations participate in N-H...O hydrogen bonding with two hydrogen phthalate anions to form a neutral unit. Both anions contain an intramolecular O-H...O hydrogen bond. In the crystal structure, these units form two-dimensional layers through [pi]-[pi] stacking interactions with a centroid-to-centroid distance of 3.763 (3) A. In turn, these layers aggregate in three dimensions by additional N-H...O hydrogen bonding. The assignment to the noncentrosymmetric space group P1 is corroborated by chemically unreasonable aromatic ring bond distances and poor K scale factor distributions for a disordered model in the centrosymmetric P\\overline{1} space group."
dc:identifierdoi:10.1107/S1600536808031681
dc:language"en"
dc:linkhttp://scripts.iucr.org/cgi-bin/paper?lh2702
dc:publisher"International Union of Crystallography"
dc:rightshttp://creativecommons.org/licenses/by/2.0/uk
dc:sourceurn:issn:1600-5368
dc:subject""
dc:title"4,4'-Iminodipyridinium bis(hydrogen phthalate)"
dc:type"text"
dcterms:abstract"In the title salt, C10H11N32+.2C8H5O4-, doubly protonated 4,4'-dipyridylamine (dpa) cations participate in N-H...O hydrogen bonding with two hydrogen phthalate anions to form a neutral unit. Both anions contain an intramolecular O-H...O hydrogen bond. In the crystal structure, these units form two-dimensional layers through [pi]-[pi] stacking interactions with a centroid-to-centroid distance of 3.763 (3) A. In turn, these layers aggregate in three dimensions by additional N-H...O hydrogen bonding. The assignment to the noncentrosymmetric space group P1 is corroborated by chemically unreasonable aromatic ring bond distances and poor K scale factor distributions for a disordered model in the centrosymmetric P\\overline{1} space group."
Author:

Name: "Robert L. LaDuca"

foaf:name"Robert L. LaDuca"
foaf:mbox"laduca@msu.edu"
rdf:typehttp://xmlns.com/foaf/0.1/Person
foaf:phonefax:+517-432-2758
ov:recordedAddress"Lyman Briggs College\nDepartment of Chemistry\nE-30 Holmes Hall\nMichigan State University\nEast Lansing\nMI 48825\nUSA"
Author:

Name: "LaDuca, Robert L."

foaf:name"LaDuca, Robert L."
ov:recordedAddress"Lyman Briggs College\nDepartment of Chemistry\nMichigan State University\nEast Lansing\nMI 48825\nUSA"
rdf:typehttp://xmlns.com/foaf/0.1/Person
Author:

Name: "Martin, David P."

foaf:name"Martin, David P."
ov:recordedAddress"Lyman Briggs College\nDepartment of Chemistry\nMichigan State University\nEast Lansing\nMI 48825\nUSA"
rdf:typehttp://xmlns.com/foaf/0.1/Person